Hexadecanoic, octadecanoic, octadec-9-enoic, octadec-9,12-dienoic and mixed fatty acids obtained from mangifera oil were converted to their methyl ester, reducing with LiAlH4 to the corresponding fatty alcohols (Ia-e). Alkyl glucosides (IIa-e) from the mentioned fatty alcohols were produced in suitable yield. The adding propylene oxide (PO) to the prepared alkyl glucosides was completed in homogeneous alkaline medium to give nonionic oxypropylated alkyl glucosides (IIIa-e), moreover, the oxypropylated alkyl glucoside was conducted to react with chlorosulphonic acid afforded oxypropylated alkyl glucoside sulphates (IVa-e) as anionic surfactants having prior surface properties to alkyl glucosides and propenoxylated derivatives. The structures of the prepared compounds were confirmed by IR and 1H NMR spectra. The surface active properties of the prepared surfactants were evaluated.