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Synthesis, characterization and magnetic properties of nanocrystalline Ni1-xZnxFe2O4 spinels via coprecipitation precursor Synthesis, characterization and magnetic properties of nanocrystalline Ni1-xZnxFe2O4 spinels via coprecipitation precursor
International Journal of Modern Physics B • 2014
Publication Information
Authors
MH Maklad, NM Shash, HK Abdelsalam
Keywords
Not Available
Journal
International Journal of Modern Physics B
Publisher
World scientific
Volume
28
Issue
25
Pages
1450165- 1450180
publication.type
International
Paper Link
Open Link
Supplementary Materials
Not Available
Abstract
Nanocrystalline Ni 1-x Zn x Fe 2 O 4 (0.0≤ x≤ 1.0) spinels are synthesized with a crystallite
size range 5–2.2 nm, using different annealing temperatures. The influence of zinc content
as well as grain size of ferrite on the ferrite microstructure, therefore on the physical
properties of ferrite, are investigated by means of X-ray diffraction (XRD), scanning electron
microscope (SEM), atomic force microscope (AFM), thermal analysis (TG, DTG, DSC) and
infrared microscopy (IR). XRD results confirm single phase spinel structure for ferrite with
size range 5–2.2 nm, using different annealing temperatures. The influence of zinc content
as well as grain size of ferrite on the ferrite microstructure, therefore on the physical
properties of ferrite, are investigated by means of X-ray diffraction (XRD), scanning electron
microscope (SEM), atomic force microscope (AFM), thermal analysis (TG, DTG, DSC) and
infrared microscopy (IR). XRD results confirm single phase spinel structure for ferrite with