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Auto-combustion synthesis and characterization of perovskite-type LaFeO3 nanocrystals prepared via different routes

Ceramics International • 2019
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Publication Information
Authors MA Gabal, F Al-Solami, YM Al Angari, AA Ali, AA Al-Juaid, Kuo-wei Huang, M Alsabban
Keywords Not Available
Journal Ceramics International
Publisher Not Available
Volume 45
Issue Not Available
Pages 16530-16539
publication.type International
Paper Link Not Available
Supplementary Materials Not Available
Abstract
LaFeO3 was prepared via simple, economical and environmentally friendly auto-combustion methods using different fuels, including citrate, urea, sucrose, egg whites, gelatin and chitosan. The prepared ferrites were systematically characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, high resolution transmission electron microscopy (HRTEM), vibrating sample magnetometry (VSM) and electrical measurements to study the impact of the synthetic routes on the various properties. XRD showed the formation of a single orthorhombic phase, except for the samples prepared via egg white, gelatin and urea methods, which indicated a secondary La2O2CO3 phase. The FT-IR and TEM studies confirmed the formation of the phase. Differential thermal analysis-thermogravimetry techniques (DTA-TG) were used to characterize the auto-combustion process up to ferrite formation. The …