| publication name | Synthesis and spectral characterization of CoxMg1−xAl2O4 as new nano-coloring agent of ceramic pigment |
|---|---|
| Authors | IS Ahmed, SA Shama, MM Moustafa, HA Dessouki, AA Ali |
| year | 2009 |
| keywords | |
| journal | Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy |
| volume | 74 |
| issue | 3 |
| pages | 665-672 |
| publisher | Elsevier |
| Local/International | International |
| Paper Link | http://www.sciencedirect.com/science/article/pii/S1386142509003436 |
| Full paper | download |
| Supplementary materials | Not Available |
Abstract
New nano-blue ceramic pigments of Co(x)Mg(1-x)Al(2)O(4) (0< or =x< or =0.1) have been prepared by co-precipitate-combustion as a hybrid method using urea as a fuel at 500 degrees C in open furnace in air atmosphere. The structure of pigment is assigned based on TGA/DTA/DrTGA analyses, X-ray diffraction (XRD) and transmission electron microscopy (TEM). Also, electronic spectra, infrared (IR) and diffuse reflectance spectroscopy (DRS) using CIE L*a*b* parameter measurement techniques were used. The results revealed that the nano-particle size of pigments were obtained in the range 30-38 nm as well as the varying colors and particle size as a result of different calcinations temperatures within the range of 500-1200 degrees C for 2h.