Synthesis of Transparent Amorphous Carbon Thin Films from Cellulose Powder in Rice Straw
Arab J Sci Eng. • 2017
Publication Information
Authors
Mahmoud Fathy· Th. Abdel Moghny· Mahmoud Ahmed Mousa ·
Abdel-Hameed A-A. El-Bellihi · Ahmed E. Awadallah
Keywords
Science
Journal
Arab J Sci Eng.
Publisher
Springer
Volume
42
Issue
Not Available
Pages
225-233
publication.type
International
Paper Link
Not Available
Supplementary Materials
Not Available
Abstract
The transparent amorphous carbon thin films
(ACTF) were prepared through a batch acid spraying technique in the presence of cobalt silicate as a catalyst at low
temperature between 30 and 45 ◦C. Hence, the catalyst was
prepared using silica gel as a basic matrix and supporting material to produce ACTF. The produced active carbon
was characterized using XRD, FTIR, and Raman spectrum.
The high-resolution transmission electron microscope (HRTEM) and thermogravimetric analysis were used to analyze
the surface morphology and thermal stability of cellulose
and ACTF, whereas the surface area was calculated using
the standard iodine method. The results of Raman spectroscopy and TEM show the realization of ACTF suspension
with highest constitutional order and the lowest number of
layers with confirming of the succeed preparation of thin
ACTF layers in thickness and average size of 1 and 100mm,
respectively.In addition, under these conditions, the activated
carbons’ iodine value is 721.64 mg/g, and the yield ratio is
85.71%
(ACTF) were prepared through a batch acid spraying technique in the presence of cobalt silicate as a catalyst at low
temperature between 30 and 45 ◦C. Hence, the catalyst was
prepared using silica gel as a basic matrix and supporting material to produce ACTF. The produced active carbon
was characterized using XRD, FTIR, and Raman spectrum.
The high-resolution transmission electron microscope (HRTEM) and thermogravimetric analysis were used to analyze
the surface morphology and thermal stability of cellulose
and ACTF, whereas the surface area was calculated using
the standard iodine method. The results of Raman spectroscopy and TEM show the realization of ACTF suspension
with highest constitutional order and the lowest number of
layers with confirming of the succeed preparation of thin
ACTF layers in thickness and average size of 1 and 100mm,
respectively.In addition, under these conditions, the activated
carbons’ iodine value is 721.64 mg/g, and the yield ratio is
85.71%
Staff Members - Benha University