Fascinating thermo-mechanical features of layered hydroxides/ MWCNTs nanocomposites
Alloys and compounds • 2019
Publication Information
Authors
M.Okil , Mohamed M.ElFaham, S.I. El-dek
Keywords
Layered hydroxides , MWCNTs,Nanocomposites,Thermal stability, Mechanical properties ,Ultrasonic velocity
Journal
Alloys and compounds
Publisher
Elsevier
Volume
788
Issue
2019
Pages
912e924
publication.type
International
Paper Link
Open Link
Supplementary Materials
Not Available
Abstract
Multiwalled carbon nanotubes (MWCNTs) has been synthesized using chemical vapor deposition (CVD)
method. Al e Layered Hydroxide (AleLH) and MWCNTs nanocomposites; (1-x) AleLH þ (x) MWCNTs,
0.0 x 1; have been synthesized using citrate nitrate assisted hydrothermal technique. The crystal
structure and the functional groups of the prepared samples were examined using X-ray diffraction
(XRD) and Infrared spectroscopy (FTIR) respectively. The layered structure seemed under the highresolution
transmission electron microscopy (HRTEM), and the morphology was observed using field
emission scanning electron microscopy (FESEM). Moreover, the synthesized nanocomposites were
further characterized using Zeta potential, size analysis and Brunauere EmmetteTeller (BET) surface area
which showed their different characteristics as the MWCNTs content is changed. Thermal gravimetric
analysis assured the thermal stability of the nanocomposites over the temperature from room up to
480 C depending on the MWCNTs content. The obtained results revealed the improvement of all mechanical
properties with the increase of MWCNTs content
method. Al e Layered Hydroxide (AleLH) and MWCNTs nanocomposites; (1-x) AleLH þ (x) MWCNTs,
0.0 x 1; have been synthesized using citrate nitrate assisted hydrothermal technique. The crystal
structure and the functional groups of the prepared samples were examined using X-ray diffraction
(XRD) and Infrared spectroscopy (FTIR) respectively. The layered structure seemed under the highresolution
transmission electron microscopy (HRTEM), and the morphology was observed using field
emission scanning electron microscopy (FESEM). Moreover, the synthesized nanocomposites were
further characterized using Zeta potential, size analysis and Brunauere EmmetteTeller (BET) surface area
which showed their different characteristics as the MWCNTs content is changed. Thermal gravimetric
analysis assured the thermal stability of the nanocomposites over the temperature from room up to
480 C depending on the MWCNTs content. The obtained results revealed the improvement of all mechanical
properties with the increase of MWCNTs content
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